Articles
1.
УДК 669.018.44:669.245
Bakradzе M.M.1, Arginbaeva E.G.1, Petrushin N.V.1, Ovsepyan S.V.1
ASPECTS OF THE DEVELOPMENT OF CASTING NICKEL AND INTERMETALLICIDE ALLOYS. TECHNOLOGY OF MANUFACTURING GTE DETAILS
The article describes the development of the direction of casting superalloys for high-temperature critical parts of gas turbine engines - the development of the first high-temperature nickel alloys with polycrystalline structure, the transition to directional and single-crystal structures, methods for calculating the chemical composition of alloys, the appearance of intermetallic and natural composite materials, manufacturing of parts from them.
Keywords: nickel alloys, intermetallic, in-situ composites, high-temperature strength.
Reference List
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4. Lashko N.F., Zaslavskaja L.V., Kozlova M.N. i dr. Fiziko-himicheskij fazovyj analiz stalej i splavov [Physical and chemical phase analysis staly and alloys]. Izd. 2-e. M.: Metallurgija, 1978. 336 s.
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13. Aviacionnye materialy. Teplofizicheskie issledovanija zharoprochnyh splavov i teplozashhitnyh pokrytij: nauch.-tehn. sb. [Aviation materials. Heatphysical researches of hot strength alloys and heat-protective coverings: scientific and technical collection] / pod obshh. red. R.E. Shalina. M.: VIAM, 1983. 132 s.
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15. Morozova G.I. Kompensacija disbalansa legirovanija zharoprochnyh nikelevyh splavov [Compensation of imbalance of alloying of heat resisting nickel alloys] // MiTOM. 2012. №12. S. 52–58.
16. Litye lopatki gazoturbinnyh dvigatelej: splavy, tehnologii, pokrytija [Cast blades of gas turbine en-gines: alloys, technologies, coverings] / pod obshh. red. E.N. Kablova. 2-e izd. M.: Nauka, 2006. 632 s.
17. Kablov E.N., Bondarenko Ju.A., Echin A.B. Razvitie tehnologii napravlennoj kristallizacii litejnyh vysokozharoprochnyh splavov s peremennym upravljaemym temperaturnym gradientom [Development of technology of cast superalloys directional solidification with variable controlled temperature gradient] // Aviacionnye materialy i tehnologii. 2017. №S. S. 24–38. DOI: 10.18577/2071-9140-2017-0-S-24-38.
18. Kablov E.N., Petrushin N.V., Bronfin M.B., Alekseev A.A. Osobennosti monokristallicheskih zharoprochnyh nikelevyh splavov, legirovannyh reniem [Features of the single-crystal heat resisting nickel alloys alloyed by reniye] // Metally. 2006. №5. S. 24–29.
19. Kablov E.N., Svetlov I.L., Petrushin N.V. Nikelevye zharoprochnye splavy, legirovannye ruteniem [The nickel hot strength alloys alloyed by ruthenium] // Aviacionnye materialy i tehnologii. M.: VIAM, 2004. Vyp.: Vysokorenievye zharoprochnye splavy, tehnologija i oborudovanie dlja proizvodstva splavov i litja monokristallicheskih turbinnyh lopatok GTD. S. 80−90.
20. Petrushin N.V., Ospennikova O.G., Svetlov I.L. Monokristallicheskie zharoprochnye nikelevye splavy dlya turbinnyh lopatok perspektivnyh GTD [Single-crystal Ni-based superalloys for turbine blades of advanced gas turbine engines] // Aviacionnye materialy i tehnologii. 2017. №S. S. 72−103. DOI: 10.18577/2071-9140-2017-0-S-72-103.
21. Petrushin N.V., Eljutin E.S., Visik E.M., Golynec S.A. Razrabotka monokristallicheskogo zharoprochnogo nikelevogo splava V pokolenija [Development of single-crystal heat resisting nickel alloy V of generation] // Metally. 2017. №6. S. 38–51.
22. Mubojadzhjan S.A., Budinovskij S.A. Ionno-plazmennaja tehnologija: perspektivnye processy, pokrytija, oborudovanie [Ion-plasma technology: prospective processes, coatings, equipment] // Aviacionnye materialy i tehnologii. 2017. №S. S. 39–54. DOI: 10.18577/2071-9140-2017-0-S-39-54.
23. Bazyleva O.A., Arginbaeva E.G., Turenko E.Yu. Vysokotemperaturnye intermetallidnye splavy dlya detaley GTD [The high-temperature intermetallic alloys for parts of gas-turbine engines] // Aviacionnye materialy i tehnologii. 2013. №3. S. 26–31.
24. Bazyleva O.A., Ospennikova O.G., Arginbaeva E.G., Letnikova E.Yu., Shestakov A.V. Tendencii razvitiya intermetallidnyh splavov na osnove nikelya [Development trends of nickel-based intermetallic alloys] // Aviacionnye materialy i tehnologii. 2017. №S. S. 104–115. DOI: 10.18577/2071-9140-2017-0-S-104-115.
25. Kachanov E.B., Petrushin N.V., Svetlov I.L. Zharoprochnye jevtekticheskie splavy s karbidno-intermetallidnym uprochneniem [Heat resisting eutectic alloys with carbide intermetallidnym hardening] // Metallovedenie i termicheskaja obrabotka metallov. 1995. №4. S. 24–29.
26. Svetlov I.L., Nejman A.V. Vlijanie temperaturno-skorostnyh parametrov napravlennoj kristallizacii na formirovanie struktury zharoprochnyh materialov [Influence of temperature and high-speed parameters of the directed crystallization on forming of structure of heat resisting materials] // Metally. 2017. №2. S. 70–75.
27. Svetlov I.L., Karpov M.I., Nejman A.V., Stroganova T.S. Temperaturnaja zavisimost predela prochnosti in-situ kompozitov mnogokomponentnoj sistemy Nb–Si–X (X=Ti, Hf, W, Cr, Al, Mo) [Temperature dependence of strength of in-situ of composites of multi-component system of Nb – Si – X-th (X=Ti, Hf, W, Cr, Al, Mo)] // Deformacija i razrushenie materialov. 2017. №10. S. 17–22.
28. Kablov E.N., Svetlov I.L., Karpov M.I., Nejman A.V., Min P.G., Karachevcev F.N. Vysokotemperaturnye kompozity na osnove sistemy Nb–Si, armirovannye silicidami niobija [High-temperature composites on the basis of the Nb-Si system, reinforced by niobium silicides] // Materialovedenie. 2017. №2. S. 24–32.
29. Sidorov V.V., Kablov D.E., Rigin V.E. Metallurgija litejnyh zharoprochnyh splavov: tehnologija i oborudovanie [Metallurgy of foundry hot strength alloys: technology and equipment] / pod obshh. red. E.N. Kablova. M.: VIAM, 2016. 368 s.
30. Nerush S.V., Evgenov A.G., Ermolaev A.S., Rogalev A.M. Issledovanie melkodispersnogo metallicheskogo poroshka zharoprochnogo splava na nikelevoj osnove dlja lazernoj LMD naplavki [Research of finely divided metal powder of hot strength alloy on nickel basis for laser LMD of welding] // Voprosy materialovedenija. 2013. №4 (76). S. 98–107.
31. Petrushin N.V., Evgenov A.G., Zavodov A.V., Treninkov I.A. Struktura i prochnost zharo-prochnogo nikelevogo splava ZhS32-VI, poluchennogo metodom selektivnogo lazernogo splavlenija na monokristallicheskoj podlozhke [Structure and durability of the heat resisting ZhS32-VI nickel alloy received by method of the selection laser fusing on single-crystal substrate] // Materialovedenie. 2017. №11. S. 19–26.
2. Kablov E.N., Ospennikova O.G., Lomberg B.S. Strategicheskie napravleniia razvitiia kon-struktsionnykh materialov i tekhnologii ikh pererabotki dlia aviatsionnykh dvigatelei nastoiashchego i budushchego [The strategic directions of development of constructional materials and technologies of their processing for aircraft engines of the present and the future] // Avtomaticheskaia svarka. 2013. №10. S. 23–32.
3. Kishkin S.T. Struktura splavov i ih prochnost [Structure of alloys and their durability] // Fizicheskie osnovy metallovedenija. M.: Gos. nauchn.-tehn. izd-vo literatury po chernoj i cvetnoj metallurgii, 1955. S. 651−704.
4. Lashko N.F., Zaslavskaja L.V., Kozlova M.N. i dr. Fiziko-himicheskij fazovyj analiz stalej i splavov [Physical and chemical phase analysis staly and alloys]. Izd. 2-e. M.: Metallurgija, 1978. 336 s.
5. Kishkin S.T. Sozdanie, issledovanie i primenenie zharoprochnyh splavov: izbrannye trudy [Creation, research and application of hot strength alloys: the chosen works]. M.: Nauka, 2006. 407 c.
6. Kishkin S.T., Kablov E.N. Litejnye zharoprochnye splavy dlja turbinnyh lopatok [Foundry hot strength alloys for turbine blades ] // Aviacionnye materialy. Izbrannye trudy «VIAM» 1932–2002. M.: MISIS–VIAM, 2002. S. 48−58.
7. Istorija aviacionnogo materialovedenija: VIAM – 75 let poiska, tvorchestva, otkrytij [History of aviation materials science: VIAM – 75 years of search, creativity, opening] / pod obshh. red. E.N. Kablova. M.: Nauka, 2007. S. 38–54.
8. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Litejnye zharoprochnye splavy novogo pokolenija [Foundry hot strength alloys of new generation] // 75 let. Aviacionnye materialy. Izbrannye trudy «VIAM» 1932–2007: jubil. nauch.-tehnich. sb. M.: VIAM, 2007. S. 27–44.
9. Samojlov A.I., Nazarkin R.M., Petrushin N.V., Moiseeva N.S. Misfit kak harakteristika urovnja mezhfaznyh naprjazhenij v monokristallicheskih zharoprochnyh nikelevyh splavah [Misfit as the characteristic of level of interphase tension in single-crystal heat resisting nickel alloys] // Metally. 2011. №3. S. 71–77.
10. Bokshtejn S.Z., Ignatova I.A., Bolberova E.V. i dr. Vlijanie nesootvetstvija parametrov reshjotok faz na diffuzionnuju pronicaemost' mezhfaznyh granic [Influence of discrepancy of parameters of grids of phases on diffusion permeability of interphase borders] // Fizika metallov i metallovedenie. 1985. T. 59. Vyp. 5. S. 936–942.
11. Samojlov A.I., Kablov E.N., Petrushin N.V., Roshhina I.N. Razmernoe nesootvetstvie kristallicheskih reshetok γ- i γʹ-faz v nikelevyh renijsoderzhashhih zharoprochnyh splavah [Dimensional discrepancy of crystal lattices γ-and γ-phases in nickel reniye containing hot strength alloys] // Litejnye zharoprochnye splavy. Jeffekt S.T. Kishkina. M.: Nauka, 2006. S. 131−141.
12. Kablov E.N., Svetlov I.L., Petrushin N.V. Nikelevye zharoprochnye splavy dlja lopatok s napravlennoj i monokristallicheskoj strukturoj (chast I) [Nickel hot strength alloys for blades with the directed and single-crystal structure (part I)] // Materialovedenie. 1997. №4. S. 32−39.
13. Aviacionnye materialy. Teplofizicheskie issledovanija zharoprochnyh splavov i teplozashhitnyh pokrytij: nauch.-tehn. sb. [Aviation materials. Heatphysical researches of hot strength alloys and heat-protective coverings: scientific and technical collection] / pod obshh. red. R.E. Shalina. M.: VIAM, 1983. 132 s.
14. Konstrukcionnye i zharoprochnye materialy dlja novoj tehniki [Constructional and heat resisting materials for new equipment]. M.: Nauka, 1978. 343 s.
15. Morozova G.I. Kompensacija disbalansa legirovanija zharoprochnyh nikelevyh splavov [Compensation of imbalance of alloying of heat resisting nickel alloys] // MiTOM. 2012. №12. S. 52–58.
16. Litye lopatki gazoturbinnyh dvigatelej: splavy, tehnologii, pokrytija [Cast blades of gas turbine en-gines: alloys, technologies, coverings] / pod obshh. red. E.N. Kablova. 2-e izd. M.: Nauka, 2006. 632 s.
17. Kablov E.N., Bondarenko Ju.A., Echin A.B. Razvitie tehnologii napravlennoj kristallizacii litejnyh vysokozharoprochnyh splavov s peremennym upravljaemym temperaturnym gradientom [Development of technology of cast superalloys directional solidification with variable controlled temperature gradient] // Aviacionnye materialy i tehnologii. 2017. №S. S. 24–38. DOI: 10.18577/2071-9140-2017-0-S-24-38.
18. Kablov E.N., Petrushin N.V., Bronfin M.B., Alekseev A.A. Osobennosti monokristallicheskih zharoprochnyh nikelevyh splavov, legirovannyh reniem [Features of the single-crystal heat resisting nickel alloys alloyed by reniye] // Metally. 2006. №5. S. 24–29.
19. Kablov E.N., Svetlov I.L., Petrushin N.V. Nikelevye zharoprochnye splavy, legirovannye ruteniem [The nickel hot strength alloys alloyed by ruthenium] // Aviacionnye materialy i tehnologii. M.: VIAM, 2004. Vyp.: Vysokorenievye zharoprochnye splavy, tehnologija i oborudovanie dlja proizvodstva splavov i litja monokristallicheskih turbinnyh lopatok GTD. S. 80−90.
20. Petrushin N.V., Ospennikova O.G., Svetlov I.L. Monokristallicheskie zharoprochnye nikelevye splavy dlya turbinnyh lopatok perspektivnyh GTD [Single-crystal Ni-based superalloys for turbine blades of advanced gas turbine engines] // Aviacionnye materialy i tehnologii. 2017. №S. S. 72−103. DOI: 10.18577/2071-9140-2017-0-S-72-103.
21. Petrushin N.V., Eljutin E.S., Visik E.M., Golynec S.A. Razrabotka monokristallicheskogo zharoprochnogo nikelevogo splava V pokolenija [Development of single-crystal heat resisting nickel alloy V of generation] // Metally. 2017. №6. S. 38–51.
22. Mubojadzhjan S.A., Budinovskij S.A. Ionno-plazmennaja tehnologija: perspektivnye processy, pokrytija, oborudovanie [Ion-plasma technology: prospective processes, coatings, equipment] // Aviacionnye materialy i tehnologii. 2017. №S. S. 39–54. DOI: 10.18577/2071-9140-2017-0-S-39-54.
23. Bazyleva O.A., Arginbaeva E.G., Turenko E.Yu. Vysokotemperaturnye intermetallidnye splavy dlya detaley GTD [The high-temperature intermetallic alloys for parts of gas-turbine engines] // Aviacionnye materialy i tehnologii. 2013. №3. S. 26–31.
24. Bazyleva O.A., Ospennikova O.G., Arginbaeva E.G., Letnikova E.Yu., Shestakov A.V. Tendencii razvitiya intermetallidnyh splavov na osnove nikelya [Development trends of nickel-based intermetallic alloys] // Aviacionnye materialy i tehnologii. 2017. №S. S. 104–115. DOI: 10.18577/2071-9140-2017-0-S-104-115.
25. Kachanov E.B., Petrushin N.V., Svetlov I.L. Zharoprochnye jevtekticheskie splavy s karbidno-intermetallidnym uprochneniem [Heat resisting eutectic alloys with carbide intermetallidnym hardening] // Metallovedenie i termicheskaja obrabotka metallov. 1995. №4. S. 24–29.
26. Svetlov I.L., Nejman A.V. Vlijanie temperaturno-skorostnyh parametrov napravlennoj kristallizacii na formirovanie struktury zharoprochnyh materialov [Influence of temperature and high-speed parameters of the directed crystallization on forming of structure of heat resisting materials] // Metally. 2017. №2. S. 70–75.
27. Svetlov I.L., Karpov M.I., Nejman A.V., Stroganova T.S. Temperaturnaja zavisimost predela prochnosti in-situ kompozitov mnogokomponentnoj sistemy Nb–Si–X (X=Ti, Hf, W, Cr, Al, Mo) [Temperature dependence of strength of in-situ of composites of multi-component system of Nb – Si – X-th (X=Ti, Hf, W, Cr, Al, Mo)] // Deformacija i razrushenie materialov. 2017. №10. S. 17–22.
28. Kablov E.N., Svetlov I.L., Karpov M.I., Nejman A.V., Min P.G., Karachevcev F.N. Vysokotemperaturnye kompozity na osnove sistemy Nb–Si, armirovannye silicidami niobija [High-temperature composites on the basis of the Nb-Si system, reinforced by niobium silicides] // Materialovedenie. 2017. №2. S. 24–32.
29. Sidorov V.V., Kablov D.E., Rigin V.E. Metallurgija litejnyh zharoprochnyh splavov: tehnologija i oborudovanie [Metallurgy of foundry hot strength alloys: technology and equipment] / pod obshh. red. E.N. Kablova. M.: VIAM, 2016. 368 s.
30. Nerush S.V., Evgenov A.G., Ermolaev A.S., Rogalev A.M. Issledovanie melkodispersnogo metallicheskogo poroshka zharoprochnogo splava na nikelevoj osnove dlja lazernoj LMD naplavki [Research of finely divided metal powder of hot strength alloy on nickel basis for laser LMD of welding] // Voprosy materialovedenija. 2013. №4 (76). S. 98–107.
31. Petrushin N.V., Evgenov A.G., Zavodov A.V., Treninkov I.A. Struktura i prochnost zharo-prochnogo nikelevogo splava ZhS32-VI, poluchennogo metodom selektivnogo lazernogo splavlenija na monokristallicheskoj podlozhke [Structure and durability of the heat resisting ZhS32-VI nickel alloy received by method of the selection laser fusing on single-crystal substrate] // Materialovedenie. 2017. №11. S. 19–26.
2.
УДК 669.017:669.018.44
Ospennikova O.G.1, L.I. Rassohina1, Bityutskaya O.N.1, Gamasina M.V.1
THE STUDY OF FOUNDRY TECHNOLOGICAL AND STRENGTH CHARACTERISTICS OF THE CAST VERSION OF ALLOY ВЖ159, IN RELATION TO THE MANUFACTURE OF SHAPED CASTINGS OF PARTS OF AIRCRAFT GAS TURBINE ENGINES
The results of studies of the technological properties of foundry and the basic strength characteristics of the cast version of alloy ВЖ159, superior in the properties of heat-resistant alloy of Nickel-chrome based ЭП648. ВЖ159 alloy has high weldability characteristics, including, in hardened condition, which ensures maintainability of parts and welded parts of it. It is concluded that the use of alloy ВЖ159 possible for the manufacture of shaped castings of parts of aircraft engines.
Keywords: alloy ВЖ159, castability, fittings, gas turbine engines, strength, linear shrinkage, volumetric shrinkage.
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7. Evgenov A.G., Rogalev A.M., Nerush S.V., Mazalov I.S. Issledovanie svojstv splava EP648, poluchennogo metodom selektivnogo lazernogo splavleniya metallicheskih poroshkov [A study of properties of EP648 alloy manufactured by the selective laser sintering of metal powders] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №2. St. 02. Available at: http://www.viam-works.ru (accessed: October 16, 2017). DOI: 10.18577/2307-6046-2015-0-2-2-2.
8. Kablov E.N., Evgenov A.G., Ospennikova O.G., Semenov B.I. i dr. Metalloporoshkovye kom-pozicii zharoprochnogo splava JeP648 proizvodstva FGUP «VIAM» GNC RF v tehnologijah selektivnogo lazernogo splavlenija, lazernoj gazoporoshkovoj naplavki i vysokotochnogo lit'ja polimerov, napolnennyh metallicheskimi poroshkami [Metalpowder compositions of EP648 hot strength alloy of production of FSUE «VIAM» SSC of RF in technologies of the selection laser fusing, laser gazoporoshkovy welding and high-precision molding of the polymers filled with metal powders] // Izvestija vuzov. Ser.: Mashinostroenie. 2016. №9 (678). S. 62–80.
9. Evgenov A.G., Rogalev A.M., Karachevcev F.N., Mazalov I.S. Vlijanie gorjachego izostatiche-skogo pressovanija i termicheskoj obrabotki na svojstva splava JeP648, sintezirovannogo metodom selektivnogo lazernogo splavlenija [Influence of hot isostatic pressing and thermal processing on properties of alloy ЭП648 synthesized by method of the selection laser fusing] // Tehnologija mashinostroenija. 2015. №9. S. 11–16.
10. Lomberg B.S., Moiseev S.A. Zharoprochnye i deformiruemye splavy dlja sovremennyh i perspektivnyh GTD [Heat resisting and deformable alloys for modern and perspective GTE] // Vse materialy. Jenciklopedicheskij spravochnik. 2007. №6. S. 2–5.
11. Solntsev S.S., Shvagireva V.V., Isaeva N.V., Soloveva G.A. Zharostojkoe pokrytie dlya zashhity vysokoprochnyh slozhnolegirovannyh nikelevyh splavov ot vysokotemperaturnoj gazovoj korrozii [High temperature coating for protection of high-strength complex alloyed of nickel alloys of high-temperature gas corrosion] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2014. №6. St. 04. Available at: http://www.viam-works.ru (accessed: October 16, 2017). DOI: 10.18577/2307-6046-2014-0-6-4-4.
12. Lomberg B.S., Kapitanenko D.V., Mazalov I.S., Bubnov M.V. Tehnologicheskie parametry poluchenija detalej holodnoj shtampovkoj iz listovyh zagotovok zharoprochnyh splavov VZh159, VZh171 i vysokoprochnogo splava VZh172 [Technological parameters of receiving details cold forming from sheet preparations of hot strength alloys VZh159, ВЖ171 and VZh172 high-strength alloy] // Kuznechno-shtampovochnoe proizvodstvo. Obrabotka materialov davleniem. 2015. №8. S. 14–19.
13. Mazalov I.S., Evgenov A.G., Prager S.M. Perspektivy primeneniya zharoprochnogo strukturnostabilnogo splava VZh159 dlya additivnogo proizvodstva vysokotemperaturnyh detalej GTD [Perspectives of heat resistant structurally stable alloy VZh159 application for additive production of high-temperature parts of GTE] // Aviacionnye materialy i tehnologii. 2016. №S1. S. 3–7. DOI: 10.18577/2071-9140-2016-0-S1-3-7.
14. Evgenov A.G., Gorbovec M.A., Prager S.M. Struktura i mehanicheskie svojstva zharoprochnyh splavov VZh159 i EP648, poluchennyh metodom selektivnogo lazernogo splavleniya [Structure and mechanical properties of heat resistant alloys VZh159 and EP648, prepared by selective laser fusing] // Aviacionnye materialy i tehnologii. 2016. №S1. S. 8–15. DOI: 10.18577/2071-9140-2016-0-S1-8-15.
15. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
2. Lomberg B.S., Ovsepjan S.V., Bakradze M.M., Mazalov I.S. Vysokozharoprochnye deformiruemye nikelevye splavy dlja perspektivnyh gazoturbinnyh dvigatelej i gazoturbinnyh ustanovok [High-heat resisting deformable nickel alloys for perspective gas turbine engines and gas turbine units] // Vestnik MGTU im. N.Je. Baumana. Ser.: Mashinostroenie. 2011. №SP2. S. 98–103.
3. Moiseev S.A., Latyshev V.B. Zharoprochnye svarivaemye splavy dlja uzlov statora sovremennyh i perspektivnyh aviacionnyh GTD [Heat resisting welded alloys for nodes of stator of modern and perspective aviation GTE] // Aviacionnye materialy i tehnologii. 2003. №1. S. 152–157.
4. Kablov E.N. Tendentsii i orientiry innovatsionnogo razvitiya Rossii [Tendencies and reference points of innovative development of Russia]: sb. nauch.-inform. mater. 3-e izd. M.: VIAM, 2015. 720 s.
5. Kablov E.N., Ospennikova O.G., Lomberg B.S., Sidorov V.V. Prioritetnye napravlenija razvitija tehnologij proizvodstva zharoprochnyh materialov dlja aviacionnogo dvigatelestroenija [The priority directions of development of production technologies of heat resisting materials for aviation engine building] // Problemy chernoj metallurgii i materialovedenija. 2013. №3. S. 47–54.
6. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Litejnye zharoprochnye nikelevye splavy dlja perspektivnyh aviacionnyh GTD [Cast heat resisting nickel alloys for perspective aviation GTE] // Tehnologija legkih splavov. 2007. №2. S. 6–16.
7. Evgenov A.G., Rogalev A.M., Nerush S.V., Mazalov I.S. Issledovanie svojstv splava EP648, poluchennogo metodom selektivnogo lazernogo splavleniya metallicheskih poroshkov [A study of properties of EP648 alloy manufactured by the selective laser sintering of metal powders] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №2. St. 02. Available at: http://www.viam-works.ru (accessed: October 16, 2017). DOI: 10.18577/2307-6046-2015-0-2-2-2.
8. Kablov E.N., Evgenov A.G., Ospennikova O.G., Semenov B.I. i dr. Metalloporoshkovye kom-pozicii zharoprochnogo splava JeP648 proizvodstva FGUP «VIAM» GNC RF v tehnologijah selektivnogo lazernogo splavlenija, lazernoj gazoporoshkovoj naplavki i vysokotochnogo lit'ja polimerov, napolnennyh metallicheskimi poroshkami [Metalpowder compositions of EP648 hot strength alloy of production of FSUE «VIAM» SSC of RF in technologies of the selection laser fusing, laser gazoporoshkovy welding and high-precision molding of the polymers filled with metal powders] // Izvestija vuzov. Ser.: Mashinostroenie. 2016. №9 (678). S. 62–80.
9. Evgenov A.G., Rogalev A.M., Karachevcev F.N., Mazalov I.S. Vlijanie gorjachego izostatiche-skogo pressovanija i termicheskoj obrabotki na svojstva splava JeP648, sintezirovannogo metodom selektivnogo lazernogo splavlenija [Influence of hot isostatic pressing and thermal processing on properties of alloy ЭП648 synthesized by method of the selection laser fusing] // Tehnologija mashinostroenija. 2015. №9. S. 11–16.
10. Lomberg B.S., Moiseev S.A. Zharoprochnye i deformiruemye splavy dlja sovremennyh i perspektivnyh GTD [Heat resisting and deformable alloys for modern and perspective GTE] // Vse materialy. Jenciklopedicheskij spravochnik. 2007. №6. S. 2–5.
11. Solntsev S.S., Shvagireva V.V., Isaeva N.V., Soloveva G.A. Zharostojkoe pokrytie dlya zashhity vysokoprochnyh slozhnolegirovannyh nikelevyh splavov ot vysokotemperaturnoj gazovoj korrozii [High temperature coating for protection of high-strength complex alloyed of nickel alloys of high-temperature gas corrosion] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2014. №6. St. 04. Available at: http://www.viam-works.ru (accessed: October 16, 2017). DOI: 10.18577/2307-6046-2014-0-6-4-4.
12. Lomberg B.S., Kapitanenko D.V., Mazalov I.S., Bubnov M.V. Tehnologicheskie parametry poluchenija detalej holodnoj shtampovkoj iz listovyh zagotovok zharoprochnyh splavov VZh159, VZh171 i vysokoprochnogo splava VZh172 [Technological parameters of receiving details cold forming from sheet preparations of hot strength alloys VZh159, ВЖ171 and VZh172 high-strength alloy] // Kuznechno-shtampovochnoe proizvodstvo. Obrabotka materialov davleniem. 2015. №8. S. 14–19.
13. Mazalov I.S., Evgenov A.G., Prager S.M. Perspektivy primeneniya zharoprochnogo strukturnostabilnogo splava VZh159 dlya additivnogo proizvodstva vysokotemperaturnyh detalej GTD [Perspectives of heat resistant structurally stable alloy VZh159 application for additive production of high-temperature parts of GTE] // Aviacionnye materialy i tehnologii. 2016. №S1. S. 3–7. DOI: 10.18577/2071-9140-2016-0-S1-3-7.
14. Evgenov A.G., Gorbovec M.A., Prager S.M. Struktura i mehanicheskie svojstva zharoprochnyh splavov VZh159 i EP648, poluchennyh metodom selektivnogo lazernogo splavleniya [Structure and mechanical properties of heat resistant alloys VZh159 and EP648, prepared by selective laser fusing] // Aviacionnye materialy i tehnologii. 2016. №S1. S. 8–15. DOI: 10.18577/2071-9140-2016-0-S1-8-15.
15. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
3.
УДК 666.7
Varrik N.M.1, Maksimov V.G.1
THE FIBROUS CERAMIC MATERIAL BASED ON ZIRCONIA FOR ALKALINE BATTERIY’S SEPARATORS
In this paper was assessing the possibility of creating a porous flexible dielectric composite material based on refractory oxide fibers for the separators of chemical power sources: alkaline batteries and fuel cells designed for power supply systems of aircraft, marine, automotive and household batteries.
It was carry out the comparative analysis of the properties of separation of materials of three kinds, proven ability of obtaining a porous composite material based on fibers of zirconium oxide having a high resistance to concentrated alkaline solution and a satisfactory mechanical strength. The investigation of obtained samples showed that the zirconia fibers with high thermal stability and chemical resistance, particularly to alkalis, have good prospects for the manufacture of separators alkaline batteries, especially in those cases where it is necessary combination of high power characteristics with increased reliability and service life.
Keywords: zirconia fiber, alkaline battery separator, a fibrous ceramic material.
Reference List
1. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
2. Tinyakova E.V., Grashhenkov D.V. Teploizolyacionnyj material na osnove mullito-korundovyh i kvarcevyh volokon [Heatinsulating material on the basis of mullit-corundum and quartz fibers] // Aviacionnye materialy i tehnologii. 2012. №3. S. 43–46.
3. Kablov E.N., Shchetanov B.V., Ivahnenko Yu.A., Balinova Yu.A. Perspektivnye armiruyushhie vysokotemperaturnye volokna dlya metallicheskih i keramicheskih kompozicionnyh materialov [Perspective reinforcing high-temperature fibers for metal and ceramic composite materials] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №2. St. 05. Available at: http://www.viam-works.ru (accessed: December 12, 2017).
4. Dospehi dlja «Burana». Materialy i tehnologii VIAM dlja MKS «Jenergija–Buran» [Armor for «Buran». Materials and VIAM technologies for ISS of «Energiya-Buran»] / pod obshh. red. E.N. Kablova. M.: Nauka i zhizn, 2013. 128 s.
5. Kablov E.N., Shhetanov B.V. Voloknistye teploizoljacionnye i teplozashhitnye materialy: svojstva, oblasti primenenija [Fibrous heatinsulating and heat-protective materials: properties, scopes] / Sb. tez. dokl. Mezhdunar. nauch.-tehnich. konf. «Fundamentalnye problemy vysokoskorostnyh techenij». Zhukovskij, 2004. S. 95–96.
6. Kablov E.N., Shhetanov B.V., Ivahnenko Ju.A., Balinova Ju.A., Semenova E.V. Volokna dioksida cirkonija dlja novogo pokolenija materialov aviacii i kosmosa [Zirconium dioxide fibers for new generation of materials of aircraft and space] / Sb. materialov 25-j Mezhdunar. konf. «Kompozicionnye materialy v promyshlennosti». Jalta, 2005. S. 320–323.
7. Zimichev A.M., Soloveva E.P. Volokno dioksida tsirkoniya dlya vysokotemperaturnogo primeneniya (obzor) [Zirconia fiber for high temperature application (review)] // Aviacionnye materialy i tehnologii. 2014. №3. S. 55–61. DOI: 10.18577/2071-9140-2014-0-3-55-61.
8. Varrik N.M., Ivahnenko Ju.A. Osobennosti poluchenija volokna oksida cirkonija (obzor) [Features of producing zirconia fibers (review)] // Trudy VIAM: jelektron. nauch. tehnich. zhurn. 2015. №10. St. 08. Available at: http://www.viam-works.ru (accessed: December 12, 2017). DOI: 10.18577/2307-6046-2015-0-10-8-8.
9. Netkanyj material dlja separatorov svincovo-kislotnyh akkumuljatornyh batarej [Nonwoven material for separators of lead-acid storage batteries]: pat. 2084049 Ros. Federacija; zajavl. 21.10.94; opubl. 10.07.97.
10. Alcaline battery separator and process of producing the same: pat. US 6037079; publ. 14.03.00.
11. Battery separator: pat. US 5336573; publ. 09.09.94.
12. Separator dlja nikel-vodorodnogo akkumuljatora [Separator for nickel - the hydrogen accumulator]: pat 2173918 Ros. Federacija; opubl. 20.09.01.
13. Flexible matrix and battery separator embodying same: pat. US 3625770; publ. 07.12.71.
14. Asbestos diaphragms for electrochemical cells and the manufacture thereof: pat. US 4367270; publ. 04.01.83.
15. Flexible battery separator and method of production: pat. US 3713890; publ. 30.01.73.
16. Multilaminate material and separator assembly for electrochemical cells: pat. US 4855196; 08.08.89.
17. Battery separator: pat. 8048556; publ. 01.11.11.
18. Zircar Zirconia Inc.: Available at: http://www.zircarzirconia.com (accessed: December 12, 2017).
19. Hamling D. Using Ceramic-Fiber Materials in Corrosive Environments // American Ceramic Society Bulletin. 1997. Vol. 76. No. 9. P. 79–82.
20. Kompozicionnyj material dlja separatora shhelochnyh akkumuljatornyh batarej [Composite material for separator of alkaline storage batteries]. pat. 2231868 Ros. Federacija; zajavl. 18.11.02; opubl. 27.06.04.
21. Kompozicionnyj material dlja separatora shhelochnyh akkumuljatornyh batarej i sposob ego poluchenija [Composite material for separator of alkaline storage batteries and way of its receiving]. pat. 2279159 Ros. Federacija; zajavl. 21.10.204; opubl. 27.06.06.
22. Sposob poluchenija poristogo kompozicionnogo materiala dlja separatorov shhelochnyh akkumuljatornyh batarej [Way of receiving porous composite material for separators of alkaline storage batteries]. pat. 2298261 Ros. Federacija; zajavl. 10.11.05; opubl. 27.04.07.
2. Tinyakova E.V., Grashhenkov D.V. Teploizolyacionnyj material na osnove mullito-korundovyh i kvarcevyh volokon [Heatinsulating material on the basis of mullit-corundum and quartz fibers] // Aviacionnye materialy i tehnologii. 2012. №3. S. 43–46.
3. Kablov E.N., Shchetanov B.V., Ivahnenko Yu.A., Balinova Yu.A. Perspektivnye armiruyushhie vysokotemperaturnye volokna dlya metallicheskih i keramicheskih kompozicionnyh materialov [Perspective reinforcing high-temperature fibers for metal and ceramic composite materials] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №2. St. 05. Available at: http://www.viam-works.ru (accessed: December 12, 2017).
4. Dospehi dlja «Burana». Materialy i tehnologii VIAM dlja MKS «Jenergija–Buran» [Armor for «Buran». Materials and VIAM technologies for ISS of «Energiya-Buran»] / pod obshh. red. E.N. Kablova. M.: Nauka i zhizn, 2013. 128 s.
5. Kablov E.N., Shhetanov B.V. Voloknistye teploizoljacionnye i teplozashhitnye materialy: svojstva, oblasti primenenija [Fibrous heatinsulating and heat-protective materials: properties, scopes] / Sb. tez. dokl. Mezhdunar. nauch.-tehnich. konf. «Fundamentalnye problemy vysokoskorostnyh techenij». Zhukovskij, 2004. S. 95–96.
6. Kablov E.N., Shhetanov B.V., Ivahnenko Ju.A., Balinova Ju.A., Semenova E.V. Volokna dioksida cirkonija dlja novogo pokolenija materialov aviacii i kosmosa [Zirconium dioxide fibers for new generation of materials of aircraft and space] / Sb. materialov 25-j Mezhdunar. konf. «Kompozicionnye materialy v promyshlennosti». Jalta, 2005. S. 320–323.
7. Zimichev A.M., Soloveva E.P. Volokno dioksida tsirkoniya dlya vysokotemperaturnogo primeneniya (obzor) [Zirconia fiber for high temperature application (review)] // Aviacionnye materialy i tehnologii. 2014. №3. S. 55–61. DOI: 10.18577/2071-9140-2014-0-3-55-61.
8. Varrik N.M., Ivahnenko Ju.A. Osobennosti poluchenija volokna oksida cirkonija (obzor) [Features of producing zirconia fibers (review)] // Trudy VIAM: jelektron. nauch. tehnich. zhurn. 2015. №10. St. 08. Available at: http://www.viam-works.ru (accessed: December 12, 2017). DOI: 10.18577/2307-6046-2015-0-10-8-8.
9. Netkanyj material dlja separatorov svincovo-kislotnyh akkumuljatornyh batarej [Nonwoven material for separators of lead-acid storage batteries]: pat. 2084049 Ros. Federacija; zajavl. 21.10.94; opubl. 10.07.97.
10. Alcaline battery separator and process of producing the same: pat. US 6037079; publ. 14.03.00.
11. Battery separator: pat. US 5336573; publ. 09.09.94.
12. Separator dlja nikel-vodorodnogo akkumuljatora [Separator for nickel - the hydrogen accumulator]: pat 2173918 Ros. Federacija; opubl. 20.09.01.
13. Flexible matrix and battery separator embodying same: pat. US 3625770; publ. 07.12.71.
14. Asbestos diaphragms for electrochemical cells and the manufacture thereof: pat. US 4367270; publ. 04.01.83.
15. Flexible battery separator and method of production: pat. US 3713890; publ. 30.01.73.
16. Multilaminate material and separator assembly for electrochemical cells: pat. US 4855196; 08.08.89.
17. Battery separator: pat. 8048556; publ. 01.11.11.
18. Zircar Zirconia Inc.: Available at: http://www.zircarzirconia.com (accessed: December 12, 2017).
19. Hamling D. Using Ceramic-Fiber Materials in Corrosive Environments // American Ceramic Society Bulletin. 1997. Vol. 76. No. 9. P. 79–82.
20. Kompozicionnyj material dlja separatora shhelochnyh akkumuljatornyh batarej [Composite material for separator of alkaline storage batteries]. pat. 2231868 Ros. Federacija; zajavl. 18.11.02; opubl. 27.06.04.
21. Kompozicionnyj material dlja separatora shhelochnyh akkumuljatornyh batarej i sposob ego poluchenija [Composite material for separator of alkaline storage batteries and way of its receiving]. pat. 2279159 Ros. Federacija; zajavl. 21.10.204; opubl. 27.06.06.
22. Sposob poluchenija poristogo kompozicionnogo materiala dlja separatorov shhelochnyh akkumuljatornyh batarej [Way of receiving porous composite material for separators of alkaline storage batteries]. pat. 2298261 Ros. Federacija; zajavl. 10.11.05; opubl. 27.04.07.
4.
category: Composite materials
УДК 620.1:678.8
Makhsidov V.V.1, Reznikov V.A.1
PROJECTS, AIMED TO DEVELOPMENT OF STRUCTURAL HEALTH MONITORING SYSTEM FOR CFRP STRUCTURES
Due to advantages fibre optic sensors base on bragg grating (FBG) begin wider and wider apply for measurement systems in some industry. Furthermore, possibilities of using FBG for remote structural health monitoring especially for aviation structural elements are estimated. In this paper method of measurement axial deformation of carbon fibre reinforced plastic (CFRP) specimen with embedded FBG during tension was studied. This method allow measuring elongation of specimens with the same precision as strain gage or extensometer. The method can apply for study of distribution of axial deformation in the CFRP specimen structure undergo to tension or compression. It is possible to use this method to measuring of axial deformation of structural elements based on CFRP which are capable to preliminary loading in operating range before operation.
Keywords: fibre optic sensor, fibre bragg grating, deformation, polymer matrix composite, CFRP, structural health monitoring.
Reference List
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2. Kablov E.N. Shestoy tekhnologicheskiy uklad [Sixth technological way] // Nauka i zhizn. 2010. №4. S. 2–7.
3. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
4. Petrov A.V., Doriomedov M.S., Skripachev S.Yu. Tehnologii utilizacii polimernyh kompozicionnyh materialov (obzor) [Recycling technologies of polymer composite materials (review)] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №8. St. 09. Available at: http://viam-works.ru (accessed: November 7, 2017). DOI: 10.18577/2307-6046-2015-0-8-9-9.
5. Erasov V.S., Yakovlev N.O., Nuzhnyj G.A. Kvalifikatsionnye ispytaniya i issledovaniya prochnosti aviatsionnyh materialov [Qualification tests and researches of durability of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 440–448.
6. Kablov E.N., Starcev O.V., Krotov A.S., Kirillov V.N. Klimaticheskoe starenie kompozicionnyh materialov aviacionnogo naznachenija. III. Znachimye faktory [Climatic aging of composite materials of aviation assignment. III. Significant factors] //Deformacija i razrushenie materialov. 2011. №1. S. 34–40.
7. Ilichev A.V., Raskutin A.E. Issledovanie vliyaniya koncentratora napryazhenij na napryazhenno-deformacionnoe sostoyanie ugleplastika metodom korrelyacii cifrovyh izobrazhenij [Research of stress concentrator influence on stress-strain state of carbon by digital images correlation method] // Aviacionnye materialy i tehnologii. 2014. №3. S. 62–66. DOI: 10.18577/2071-9140-2014-0-3-26-30.
8. Startsev V.O., Mahonkov A.Yu., Kotova E.A. Mehanicheskie svojstva i vlagostojkost' PKM s povrezhdeniyami [Mechanical properties and moisture resistance of PCM with damages] // Aviacionnye materialy i tehnologii. 2015. №S1 (38). S. 49–55. DOI: 10.18577/2071-9140-2015-0-S1-49-55.
9. Molent L., Agius J. Agile Military Aircraft // Encyclopedia of Structural Health Monitoring. John Wiley Sons, Ltd., 2009. P. 1–15.
10. Childers B.A., Froggatt M.E., Allison S.G. et al. Use of 3000 Bragg Grating Strain Sensors Distributed on Four Eight-Meter Optical Fibers During Static Load Tests of a Composite Structure // Proc. Smart Structures and Materials 2001: Industrial and Commercial Applications of Smart Structures Technologies, 2001. P. 133–142.
11. Vasilev S.A., Medvedkov I.O., Korolev I.G. i dr. Volokonnye reshetki pokazatelja prelomlenija i ih primenenie [Fiber grids of refraction index and their application] // Kvantovaja jelektronika. 2005. T. 35. №12. S. 1085–1103.
12. Sposob izmerenija deformacii konstrukcii iz kompozicionnogo materiala [Way of measurement of deformation of design from composite material]: pat. 2427795 Ros. Federacija; opubl. 03.12.09.
13. Takeda N., Tajima N., Sakurai T., Kishi T. Recent advances in composite fuselage demonstration program for damage and health monitoring in Japan // Structural control and health monitoring. 2005. Vol. 12. R. 245–255.
14. Mizutani T., Takeda N., Takeya H. On-board Strain Measurement of a Cryogenic Composite Tank Mounted on a Reusable Rocket using FBG Sensors // Structural Health Monitoring. 2006. Vol. 5. P. 205–214.
15. Adams C. HUMS Technology // Avionics Magazine. Available at: http://www.aviationtoday.com/av/military/HUMS-technology_76209.html#.VXbcJtLtlBc (accessed: November 7, 2017).
16. Proekt «SARISTU» [SARISTU project] – «Smart Intelligent Aircraft Structures»: ofic. sajt. Available at: www.saristu.eu (accessed: November 7, 2017).
17. Takeda N., Okabe Y., Kuwahara J., Kojima S., Ogisu T. Development of smart composite structures with small-diameter fiber Bragg grating sensors for damage detection: Quantitative evaluation of delamination length in CFRP laminates using Lamb wave sensing // Composites Science and Technology. 2005. Vol. 65. P. 2575–2587.
18. Takeda N. Fiber optic sensor-based SHM technologies for aerospace applications in Japan // Proc. SPIE 6933 «Smart Sensor Phenomena, Technology, Networks, and Systems». 2008. DOI: 10.1117/12.776838.
2. Kablov E.N. Shestoy tekhnologicheskiy uklad [Sixth technological way] // Nauka i zhizn. 2010. №4. S. 2–7.
3. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
4. Petrov A.V., Doriomedov M.S., Skripachev S.Yu. Tehnologii utilizacii polimernyh kompozicionnyh materialov (obzor) [Recycling technologies of polymer composite materials (review)] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №8. St. 09. Available at: http://viam-works.ru (accessed: November 7, 2017). DOI: 10.18577/2307-6046-2015-0-8-9-9.
5. Erasov V.S., Yakovlev N.O., Nuzhnyj G.A. Kvalifikatsionnye ispytaniya i issledovaniya prochnosti aviatsionnyh materialov [Qualification tests and researches of durability of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 440–448.
6. Kablov E.N., Starcev O.V., Krotov A.S., Kirillov V.N. Klimaticheskoe starenie kompozicionnyh materialov aviacionnogo naznachenija. III. Znachimye faktory [Climatic aging of composite materials of aviation assignment. III. Significant factors] //Deformacija i razrushenie materialov. 2011. №1. S. 34–40.
7. Ilichev A.V., Raskutin A.E. Issledovanie vliyaniya koncentratora napryazhenij na napryazhenno-deformacionnoe sostoyanie ugleplastika metodom korrelyacii cifrovyh izobrazhenij [Research of stress concentrator influence on stress-strain state of carbon by digital images correlation method] // Aviacionnye materialy i tehnologii. 2014. №3. S. 62–66. DOI: 10.18577/2071-9140-2014-0-3-26-30.
8. Startsev V.O., Mahonkov A.Yu., Kotova E.A. Mehanicheskie svojstva i vlagostojkost' PKM s povrezhdeniyami [Mechanical properties and moisture resistance of PCM with damages] // Aviacionnye materialy i tehnologii. 2015. №S1 (38). S. 49–55. DOI: 10.18577/2071-9140-2015-0-S1-49-55.
9. Molent L., Agius J. Agile Military Aircraft // Encyclopedia of Structural Health Monitoring. John Wiley Sons, Ltd., 2009. P. 1–15.
10. Childers B.A., Froggatt M.E., Allison S.G. et al. Use of 3000 Bragg Grating Strain Sensors Distributed on Four Eight-Meter Optical Fibers During Static Load Tests of a Composite Structure // Proc. Smart Structures and Materials 2001: Industrial and Commercial Applications of Smart Structures Technologies, 2001. P. 133–142.
11. Vasilev S.A., Medvedkov I.O., Korolev I.G. i dr. Volokonnye reshetki pokazatelja prelomlenija i ih primenenie [Fiber grids of refraction index and their application] // Kvantovaja jelektronika. 2005. T. 35. №12. S. 1085–1103.
12. Sposob izmerenija deformacii konstrukcii iz kompozicionnogo materiala [Way of measurement of deformation of design from composite material]: pat. 2427795 Ros. Federacija; opubl. 03.12.09.
13. Takeda N., Tajima N., Sakurai T., Kishi T. Recent advances in composite fuselage demonstration program for damage and health monitoring in Japan // Structural control and health monitoring. 2005. Vol. 12. R. 245–255.
14. Mizutani T., Takeda N., Takeya H. On-board Strain Measurement of a Cryogenic Composite Tank Mounted on a Reusable Rocket using FBG Sensors // Structural Health Monitoring. 2006. Vol. 5. P. 205–214.
15. Adams C. HUMS Technology // Avionics Magazine. Available at: http://www.aviationtoday.com/av/military/HUMS-technology_76209.html#.VXbcJtLtlBc (accessed: November 7, 2017).
16. Proekt «SARISTU» [SARISTU project] – «Smart Intelligent Aircraft Structures»: ofic. sajt. Available at: www.saristu.eu (accessed: November 7, 2017).
17. Takeda N., Okabe Y., Kuwahara J., Kojima S., Ogisu T. Development of smart composite structures with small-diameter fiber Bragg grating sensors for damage detection: Quantitative evaluation of delamination length in CFRP laminates using Lamb wave sensing // Composites Science and Technology. 2005. Vol. 65. P. 2575–2587.
18. Takeda N. Fiber optic sensor-based SHM technologies for aerospace applications in Japan // Proc. SPIE 6933 «Smart Sensor Phenomena, Technology, Networks, and Systems». 2008. DOI: 10.1117/12.776838.
5.
category: Composite materials
УДК 620.1:678.8
Makhsidov V.V.1, Mukhametov R.R.1
AN EFFECT OF FIBRE OPTIC COATING ON PRECISION OF MATERIAL’S STRAIN MEASUREMENT WITH EMBEDDED FIBRE BRAGG GRATING
Due to advantages fibre optic sensors based on Bragg grating (FBG) begin wider and wider apply for measurement systems in some industry. Furthermore, possibilities of using FBG for structural health monitoring especially for aviation structural elements are estimated. Integrating elements, for example fibre optic sensors, in composite material lead to occurrence of additional boundary. As a result there are occurrence structural inhomogeneity and decrease in strength, that is a reason for reduction in mechanical properties of composite. In this paper method of measurement axial deformation of carbon fibre reinforced plastic (CFRP) specimen with embedded FBG during tension was studied. Also an effect of fibre optic coating on precision of material’s strain measurement with embedded FBG are shown. This method allow measuring elongation of specimens with the same precision as strain gage or extensometer.
Keywords: fibre optic sensor, fibre Bragg grating, deformation, polymer matrix composite, fibre cladding, adhesion.
Reference List
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2. Panin S.V., Startsev O.V., Krotov A.S. Diagnostika nachalnoj stadii klimaticheskogo stareniya PKM po izmeneniyu koefficienta diffuzii vlagi [Initial stage environmental degradation of the polymer matrix composites evaluated by Water diffusion coefficient] // Trudy VIAM: electron. nauch.-tehnich. zhurn. 2014. №7. St. 09. Available at: http://viam-works.ru (accessed: November 8, 2017). DOI: 10.18577/2307-6046-2014-0-7-9-9.
3. Kablov E.N. Shestoy tekhnologicheskiy uklad [Sixth technological way] // Nauka i zhizn. 2010. №4. S. 2–7.
4. Dimitrienko Ju.I., Gubareva E.A., Sborshhikov S.V., Erasov V.S., Jakovlev N.O. Chislennoe modelirovanie i jeksperimental'noe issledovanie deformirovanija uprugoplasticheskih plastin pri smjatii [Numerical modeling and pilot study of deformation of elasto-plastic plates when crushing] // Matematicheskoe modelirovanie i chislennye metody. 2015. №1 (5). S. 67–82.
5. Erasov V.S., Yakovlev N.O., Nuzhnyj G.A. Kvalifikatsionnye ispytaniya i issledovaniya prochnosti aviatsionnyh materialov [Qualification tests and researches of durability of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 440–448.
6. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
7. Gulyaev I.N., Gunyaev G.M., Raskutin A.E. Polimernye kompozitsionnye materialy s funktsiyami adaptacii i diagnostiki sostoianiya [Polymeric composite materials with functions of adaptation and condition diagnostics] // Aviacionnye materialy i tehnologii. 2012. №S. S. 242–253.
8. Gulyaev I.N., Gunyaev G.M. Ispolzovanie nepreryvnyh armiruyushhih volokon v kachestve tenzorezistornyh sensornyh elementov [Use of continuous reinforcing fibers as strain gauge sensing elements] // Aviacionnye materialy i tehnologii. 2010. №2. S. 22–27.
9. Kablov E.N., Sivakov D.V., Gulyaev I.N., Sorokin K.V., Fedotov M.Yu., Goncharov V.A. Metody issledovaniya konstrukcionnyh kompozicionnyh materialov s integrirovannoj elektromehanicheskoj sistemoj [Methods of research of constructional composite materials with the integrated electromechanical system] //Aviacionnye materialy i tehnologii. 2010. №4. S. 17–20.
10. Vasilev S.A., Medvedkov I.O., Korolev I.G. i dr. Volokonnye reshetki pokazatelja prelomlenija i ih primenenie [Fiber grids of refraction index and their application] // Kvantovaja jelektronika. 2005. T. 35. №12. S. 1085–1103.
11. Sposob izmerenija deformacii konstrukcii iz kompozicionnogo materiala [Way of measurement of deformation of design from composite material]: pat. 2427795 Ros. Federacija; opubl. 03.12.09.
12. Kersey A.D., Davis M.A., Patrick H.J. et al. Fiber grating sensors // J. Lightwave Technol. 1997. Vol. 15. P. 1442–1463.
13. Takeda N. Fiber optic sensor-based SHM technologies for aerospace applications in Japan // Proc. SPIE 6933 «Smart Sensor Phenomena, Technology, Networks, and Systems». 2008.
14. Takeda N., Tajima N., Sakurai T., Kishi T. Recent advances in composite fuselage demonstration program for damage and health monitoring in Japan // Structural control and health monitoring. 2005. Vol. 12. R. 245–255.
15. Childers B.A., Froggatt M.E., Allison S.G. et al. Use of 3000 Bragg grating strain sensors distributed on four 8-m optical fibers during static load tests of a composite structure // Proc. SPIE 4332 «Smart Structures and Materials–2001»: Industrial and Commercial Applications of Smart Structures Technologies. 2001. R. 133–142.
16. Hill K.O., Meltz G. Fiber Bragg grating technology fundamentals and overview //J. Lightwave Technol. 1997. Vol. 15. P. 1263–1276.
17. Mahsidov V.V., Fedotov M.Ju., Shienok A.M., Zuev M.A. K voprosu ob integracii optovolokna v PKM i izmerenii deformacii materiala s pomoshhju volokonnyh brjeggovskih reshetok [To question of integration of optical fiber in PCM and measurement of deformation of material by means of fiber Bragg grids] // Mehanika kompozicionnyh materialov i konstrukcij. 2014. T. 20. №4. S. 568–584.
18. Mahsidov V.V., Jakovlev N.O., Ilichev A.V., Shienok A.M. Izmerenie deformacii ugleplastika s pomoshh'ju integrirovannyh v ego strukturu volokonnyh brjeggovskih reshetok [Deformation measurement ugleplastika by means of the fiber Bragg grids integrated into its structure] // Mehanika kompozicionnyh materialov i konstrukcij. 2015. T. 21. №3. S. 360–369.
19. Roberts S.S.J., Davidson R. Mechanical properties of composite materials containing embedded fiber-optic sensors // Proc. SPIE «Fiber Optic Smart Structures and Skins IV». 1991. DOI: 10.1117/12.50193.
20. Leduc D., Lecieux Y., Morvan P.-A., Lupi C. Architecture of optical fiber sensor for the simultaneous measurement of axial and radial strains // Smart Mater. Struct. 2013. Vol. 22. P. 9.
21. Bertholds A., Dandliker R. Determination of the individual strain-optic coefficients in single-mode optical fibers // J. Lightwave Technol. 1988. Vol. 6. P. 17–20.
2. Panin S.V., Startsev O.V., Krotov A.S. Diagnostika nachalnoj stadii klimaticheskogo stareniya PKM po izmeneniyu koefficienta diffuzii vlagi [Initial stage environmental degradation of the polymer matrix composites evaluated by Water diffusion coefficient] // Trudy VIAM: electron. nauch.-tehnich. zhurn. 2014. №7. St. 09. Available at: http://viam-works.ru (accessed: November 8, 2017). DOI: 10.18577/2307-6046-2014-0-7-9-9.
3. Kablov E.N. Shestoy tekhnologicheskiy uklad [Sixth technological way] // Nauka i zhizn. 2010. №4. S. 2–7.
4. Dimitrienko Ju.I., Gubareva E.A., Sborshhikov S.V., Erasov V.S., Jakovlev N.O. Chislennoe modelirovanie i jeksperimental'noe issledovanie deformirovanija uprugoplasticheskih plastin pri smjatii [Numerical modeling and pilot study of deformation of elasto-plastic plates when crushing] // Matematicheskoe modelirovanie i chislennye metody. 2015. №1 (5). S. 67–82.
5. Erasov V.S., Yakovlev N.O., Nuzhnyj G.A. Kvalifikatsionnye ispytaniya i issledovaniya prochnosti aviatsionnyh materialov [Qualification tests and researches of durability of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 440–448.
6. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
7. Gulyaev I.N., Gunyaev G.M., Raskutin A.E. Polimernye kompozitsionnye materialy s funktsiyami adaptacii i diagnostiki sostoianiya [Polymeric composite materials with functions of adaptation and condition diagnostics] // Aviacionnye materialy i tehnologii. 2012. №S. S. 242–253.
8. Gulyaev I.N., Gunyaev G.M. Ispolzovanie nepreryvnyh armiruyushhih volokon v kachestve tenzorezistornyh sensornyh elementov [Use of continuous reinforcing fibers as strain gauge sensing elements] // Aviacionnye materialy i tehnologii. 2010. №2. S. 22–27.
9. Kablov E.N., Sivakov D.V., Gulyaev I.N., Sorokin K.V., Fedotov M.Yu., Goncharov V.A. Metody issledovaniya konstrukcionnyh kompozicionnyh materialov s integrirovannoj elektromehanicheskoj sistemoj [Methods of research of constructional composite materials with the integrated electromechanical system] //Aviacionnye materialy i tehnologii. 2010. №4. S. 17–20.
10. Vasilev S.A., Medvedkov I.O., Korolev I.G. i dr. Volokonnye reshetki pokazatelja prelomlenija i ih primenenie [Fiber grids of refraction index and their application] // Kvantovaja jelektronika. 2005. T. 35. №12. S. 1085–1103.
11. Sposob izmerenija deformacii konstrukcii iz kompozicionnogo materiala [Way of measurement of deformation of design from composite material]: pat. 2427795 Ros. Federacija; opubl. 03.12.09.
12. Kersey A.D., Davis M.A., Patrick H.J. et al. Fiber grating sensors // J. Lightwave Technol. 1997. Vol. 15. P. 1442–1463.
13. Takeda N. Fiber optic sensor-based SHM technologies for aerospace applications in Japan // Proc. SPIE 6933 «Smart Sensor Phenomena, Technology, Networks, and Systems». 2008.
14. Takeda N., Tajima N., Sakurai T., Kishi T. Recent advances in composite fuselage demonstration program for damage and health monitoring in Japan // Structural control and health monitoring. 2005. Vol. 12. R. 245–255.
15. Childers B.A., Froggatt M.E., Allison S.G. et al. Use of 3000 Bragg grating strain sensors distributed on four 8-m optical fibers during static load tests of a composite structure // Proc. SPIE 4332 «Smart Structures and Materials–2001»: Industrial and Commercial Applications of Smart Structures Technologies. 2001. R. 133–142.
16. Hill K.O., Meltz G. Fiber Bragg grating technology fundamentals and overview //J. Lightwave Technol. 1997. Vol. 15. P. 1263–1276.
17. Mahsidov V.V., Fedotov M.Ju., Shienok A.M., Zuev M.A. K voprosu ob integracii optovolokna v PKM i izmerenii deformacii materiala s pomoshhju volokonnyh brjeggovskih reshetok [To question of integration of optical fiber in PCM and measurement of deformation of material by means of fiber Bragg grids] // Mehanika kompozicionnyh materialov i konstrukcij. 2014. T. 20. №4. S. 568–584.
18. Mahsidov V.V., Jakovlev N.O., Ilichev A.V., Shienok A.M. Izmerenie deformacii ugleplastika s pomoshh'ju integrirovannyh v ego strukturu volokonnyh brjeggovskih reshetok [Deformation measurement ugleplastika by means of the fiber Bragg grids integrated into its structure] // Mehanika kompozicionnyh materialov i konstrukcij. 2015. T. 21. №3. S. 360–369.
19. Roberts S.S.J., Davidson R. Mechanical properties of composite materials containing embedded fiber-optic sensors // Proc. SPIE «Fiber Optic Smart Structures and Skins IV». 1991. DOI: 10.1117/12.50193.
20. Leduc D., Lecieux Y., Morvan P.-A., Lupi C. Architecture of optical fiber sensor for the simultaneous measurement of axial and radial strains // Smart Mater. Struct. 2013. Vol. 22. P. 9.
21. Bertholds A., Dandliker R. Determination of the individual strain-optic coefficients in single-mode optical fibers // J. Lightwave Technol. 1988. Vol. 6. P. 17–20.
6.
УДК 621.792.053:678.046.3
Petrova A.P.1, Lukina N.Ph.1, Pavlyuk B.F.1, Isaev A.Yu.1, Besednov K.L.1
FILLERS FOR CONDUCTING GLUES (literature review)
The review of scientific and technical literature and patents on fillers used in the composition of conductive adhesives to give them the properties of electrical conductivity. For compile this review, a search, selection, systematization and analysis of scientific, technical and patent literature by countries: Russia, USA, Japan, Germany, France, Great Britain and China, has been carried out. Retrospective search was 27 years. The most commonly fillers used in the conductive adhesives, the advantages and disadvantages of each of the fillers, the level of electrical conductivity achieved is determined. The influence of form of the filler particles on the electrical conductivity is shown.
Keywords: filler, conductivity, the conducting composition, electro carrying-out adhesive, silver powder, unit volume electrical resistance, filler structure.
Reference List
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3. Conductive adhesive and article made therewith: pat. 5173765 А USA; publ. 22.12.92.
4. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
5. Kablov E.N. Strategicheskie napravleniya razvitiya materialov i tekhnologiy ikh pererabotki na period do 2030 goda [The strategic directions of development of materials and technologies of their processing for the period till 2030] // Aviatsionnye materialy i tekhnologii. 2012. №S. S. 7–17.
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9. Conductive adhesive and method for mounting electronic part using same: pat. 3681907 В2 JP; publ. 10.08.05.
10. Conductive adhesive composition: pat. 7345105 В2 USA; publ. 18.03.08.
11. Conductive resin compositions and electronic parts using the same: pat. 6680007 В2 USA;
publ. 20.01.2004.
12. Conductive adhesive and circuit using the same: app. 2005/0230667 А1 USA; publ. 20.10.05.
13. Conductive adhesive: app. EP 2042580 А1; publ. 01.04.09.
14. Electroconductive paste: app. EP 2911160 А1; publ. 26.08.15.
15. Thermosetting type conductive paste and laminated ceramic electronic component having an external electrode formed by using such thermosetting type conductive paste: app. 1965397 А1 EP; publ. 03.09.08.
16. Conductive paste, laminated ceramic component, printed circuit board, and electronic device: pat. 3121819 А1 EP; publ. 25.01.17.
17. High thermally conductive polymeric adhesive: pat. 6265471 В1 USA; publ. 24.07.01.
18. Adhesives With Thermal Conductivity Enhanced By Mixed Silver Fillers: pat. 8795837 В2 USA; publ. 05.08.14.
19. Conductive adhesives comprising silver-coated particles: app. 2014178671 A1 USA; publ. 26.06.14.
20. Conductive inks and pastes: app. 2010009153 А1 USA; publ. 14.01.10.
21. Silver conductive adhesive and preparation: pat. 9567496 В2 USA; publ. 14.02.17.
22. Highly conductive electrically conductive: pat. 9490043 В2; publ. 08.11.16.
23. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2408642 S1 Ros. Federatsiia; 10.01.11, Biul. №1.
24. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2246519 S2 Ros. Federatsiia; 20.02.05, Biul. №5.
25. Conductive adhesive: app. 2010/0044088 А1 USA; publ. 25.02.10.
26. Polymeric adhesive: app. 6140402 А USA; publ. 31.10.00.
27. Adhesive paste containing polymeric resin: pat. 0719299 В1 EP; publ. 14.11.01.
28. Electroconductive adhesive: pat. 2748615 B2 USA; publ. 11.02.92.
29. Electrically conductive adhesives and methods of making: pat. 7527749 В2 USA; publ. 05.05.09.
30. Flexible microelectronics adhesive: app. 2010/219526 А1 USA; publ. 02.09.10.
31. Die attach adhesive compositions: app. 6147141 А USA, publ. 14.11.00.
32. Snap-cure epoxy adhesives: app. 5770706 А USA; publ. 23.06.98.
33. Silver coated flaky material filled conductive curable composition and the application in die:
app. 20110095241 А1 USA; publ. 28.04.11.
34. Electrically conductive: app. 20160035910 А1 USA; publ. 04.02.16.
35. Sinterable silver flake adhesive for use in electronics: app. 2013/0187102 А1 USA; publ. 25.07.13.
36. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2058361 S1 Ros. Federatsiia; 20.04.96.
37. Conductive adhesive and the semiconductor device: pat. 2893782 В2 JP; publ. 24.05.99.
38. Electrically conductive adhesive composition, electrically conductive adhesive sheet and use thereof: pat. 6344155 В1 USA; publ. 05.02.02.
39. Electrically conductive adhesive: pat. 2748615 В2 JP; publ. 18.07.91.
40. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2308105 S1 Ros. Federatsiia; 10.10.07, Biul. №28.
41. Carbon nanotube composite structure and adhesive member: app. 2011077784 А1, WO; publ. 30.06.11.
2. Petrova A.P., Lukina N.F. Klei dlia mnogorazovoi kosmicheskoi sistemy [Adhesives for «Вuran» reusable spaceship] //Aviatsionnye materialy i tekhnologii. 2013. №S1. S. 131–136.
3. Conductive adhesive and article made therewith: pat. 5173765 А USA; publ. 22.12.92.
4. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
5. Kablov E.N. Strategicheskie napravleniya razvitiya materialov i tekhnologiy ikh pererabotki na period do 2030 goda [The strategic directions of development of materials and technologies of their processing for the period till 2030] // Aviatsionnye materialy i tekhnologii. 2012. №S. S. 7–17.
6. Kablov E.N. Kontrol kachestva materialov – garantiya bezopasnosti ekspluatatsii aviatsionnoy tekhniki [Quality control of materials – security accreditation of operation of aviation engineering] // Aviatsionnye materialy i tekhnologii. 2001. №1. S. 3–8.
7. Kablov E.N. Aviatsionnoe materialovedenie v XXI veke. Perspektivy i zadachi [Aviation materials science in the XXI century. Perspectives and tasks] // Aviatsionnye materialy. Izbrannye trudy «VIAM» 1932–2002. M.: VIAM, 2002. S. 23–47.
8. Grashhenkov D.V., Chursova L.V. Strategiya razvitiya kompozicionnyh i funkcionalnyh materialov [Strategy of development of composite and functional materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 231–242.
9. Conductive adhesive and method for mounting electronic part using same: pat. 3681907 В2 JP; publ. 10.08.05.
10. Conductive adhesive composition: pat. 7345105 В2 USA; publ. 18.03.08.
11. Conductive resin compositions and electronic parts using the same: pat. 6680007 В2 USA;
publ. 20.01.2004.
12. Conductive adhesive and circuit using the same: app. 2005/0230667 А1 USA; publ. 20.10.05.
13. Conductive adhesive: app. EP 2042580 А1; publ. 01.04.09.
14. Electroconductive paste: app. EP 2911160 А1; publ. 26.08.15.
15. Thermosetting type conductive paste and laminated ceramic electronic component having an external electrode formed by using such thermosetting type conductive paste: app. 1965397 А1 EP; publ. 03.09.08.
16. Conductive paste, laminated ceramic component, printed circuit board, and electronic device: pat. 3121819 А1 EP; publ. 25.01.17.
17. High thermally conductive polymeric adhesive: pat. 6265471 В1 USA; publ. 24.07.01.
18. Adhesives With Thermal Conductivity Enhanced By Mixed Silver Fillers: pat. 8795837 В2 USA; publ. 05.08.14.
19. Conductive adhesives comprising silver-coated particles: app. 2014178671 A1 USA; publ. 26.06.14.
20. Conductive inks and pastes: app. 2010009153 А1 USA; publ. 14.01.10.
21. Silver conductive adhesive and preparation: pat. 9567496 В2 USA; publ. 14.02.17.
22. Highly conductive electrically conductive: pat. 9490043 В2; publ. 08.11.16.
23. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2408642 S1 Ros. Federatsiia; 10.01.11, Biul. №1.
24. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2246519 S2 Ros. Federatsiia; 20.02.05, Biul. №5.
25. Conductive adhesive: app. 2010/0044088 А1 USA; publ. 25.02.10.
26. Polymeric adhesive: app. 6140402 А USA; publ. 31.10.00.
27. Adhesive paste containing polymeric resin: pat. 0719299 В1 EP; publ. 14.11.01.
28. Electroconductive adhesive: pat. 2748615 B2 USA; publ. 11.02.92.
29. Electrically conductive adhesives and methods of making: pat. 7527749 В2 USA; publ. 05.05.09.
30. Flexible microelectronics adhesive: app. 2010/219526 А1 USA; publ. 02.09.10.
31. Die attach adhesive compositions: app. 6147141 А USA, publ. 14.11.00.
32. Snap-cure epoxy adhesives: app. 5770706 А USA; publ. 23.06.98.
33. Silver coated flaky material filled conductive curable composition and the application in die:
app. 20110095241 А1 USA; publ. 28.04.11.
34. Electrically conductive: app. 20160035910 А1 USA; publ. 04.02.16.
35. Sinterable silver flake adhesive for use in electronics: app. 2013/0187102 А1 USA; publ. 25.07.13.
36. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2058361 S1 Ros. Federatsiia; 20.04.96.
37. Conductive adhesive and the semiconductor device: pat. 2893782 В2 JP; publ. 24.05.99.
38. Electrically conductive adhesive composition, electrically conductive adhesive sheet and use thereof: pat. 6344155 В1 USA; publ. 05.02.02.
39. Electrically conductive adhesive: pat. 2748615 В2 JP; publ. 18.07.91.
40. Tokoprovodiashchaia kleevaia kompozitsiia [Conducting glue composition]: pat. 2308105 S1 Ros. Federatsiia; 10.10.07, Biul. №28.
41. Carbon nanotube composite structure and adhesive member: app. 2011077784 А1, WO; publ. 30.06.11.
7.
УДК 665.939.5
Petrova A.P.1
INFLUENCE OF СARBORANE GROUPS ON CURING PROCESSES OF CARBORANE-CONTAINING ADHESIVES OF DIFFERENT CHEMICAL NATURE
Part 2. Curing of the carboranconteined polyurethane and siloxane adhesive
Mechanisms of curing of glues as a part of which carboranconteined components are used are considered. Curing processes in сarboranconteined, polyurethane and siloxane adhesive are investigated. Researches carried out using methods IR-spectrum, TGA and on change of the maintenance of soluble fraction in cured compositions. Influence of structure of сarborane groups on curing processes is shown.
Results of experiments on decrease in temperature of curing of сarboranconteined glue compositions are given.
Keywords: carboranes, polyurethane, siloxane, adhesive, curing, curing catalysts, IK spektry, TGA, durability of glued joints, thermomechanical characteristics, dilatometry, x-ray diffraction analysis, diffractogram.
Reference List
1. Grajms R. Karborany [Carboranes]. Per. s angl. / pod red. A.F. Zhigacha. M.: Mir, 1974. 264 s.
2. Petrova A.P. Povyshenie termostojkosti poliuretanovyh klejashhih sistem pri modifikacii karboranami [Increase of thermal stability of polyurethane gluing systems when updating by carboranes] // Novosti materialovedenija. Nauka i tehnika: jelektron. nauch.-tehnich. zhurn. 2017. №1. St. 04. Available at: http://www.materialsnews.ru (accessed: June 27, 2017).
3. Petrova A.P., Laptev A.B. Termicheskaja ustojchivost karboransoderzhashhih poliuretanovyh klejashhih sistem [Thermal stability carborane of containing polyurethane gluing systems] // Klei. Germetiki. Tehnologii. 2017. №8. S. 2–5.
4. Lipatova T.Je., Bakalo L.A. Kinetika i mehanizm reakcij obrazovanija poliuretanov [Kinetics and mechanism of reactions of education poliuretanov] // Uspehi himii poliuretanov. Kiev: Naukova Dumka, 1972. S. 195–213.
5. Valeckij P.M., Petrova A.P. Polimernye klei na osnove karboransoderzhashhih soedinenij [Polymeric glues on basis carborane of containing connections] // Klei. Germetiki. Tehnologii. 2005. №3. S. 2–5.
6. Lukina N.F., Dementeva L.A., Petrova A.P., Serezhenkov A.A. Konstrukcionnye i termostojkie klei [Constructional and heat-resistant glues] // Aviacionnye materialy i tehnologii. 2012. №S. S. 328–335.
7. Sharova I.A., Petrova A.P. Obzor po materialam mezhdunarodnoj konferencii po kleyam i germetikam (WAC-2012, Franciya) [Review of world adhesive and sealant conference (WAC-2012, France] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №8. St. 06. Available at: http://www.viam-works.ru (accessed: June 19, 2017).
8. Petrova A.P. Magnitoprovodjashhie kleevye kompozicii na osnove karboransoderzhashhih soedinenij [Magneto carrying-out glue compositions on basis carborane of containing connections] // Klei. Germetiki. Tehnologii. 2006. №11. S. 3–4.
9. Petrova A.P. Povyshenie termostojkosti klejashhih sistem na osnove fenolformaldegidnyh oligomerov pri modifikacii karboranami [Increasing thermal resistance of the adhesive systems based on phenol-formaldehyde oligomers with modification of the carborane] // Novosti materialovedenija. Nauka i tehnika: jelektron. nauch.-tehnich. zhurn. 2017. №1. St. 03. Available at: http://www.materialsnews.ru (accessed: June 27, 2017).
10. Petrova A.P. Laptev A.B. Termicheskaja ustojchivost karboransoderzhashhih klejashhih sistem na osnove fenolformaldegidnyh oligomerov [Thermal stability of karboransoderzhashchy gluing systems on the basis of fenolformaldegidny oligomers] // Klei. Germetiki. Tehnologii. 2017. №7. S. 2–6.
11. Petrova A.P., Laptev A.B. Fenolno-kauchukovye klei, modificirovannye karboranami [The phenolic and rubber glues modified by carboranes] // Klei. Germetiki. Tehnologii. 2017. №6. S. 2–6.
12. Petrova A.P., Valeckij P.M. Fenolno-kauchukovye karboransoderzhashhie klei s sobstvennym fer-romagnetizmom [Phenolic and rubber carborane containing glues with own ferromagnetizm] // Klei. Germetiki. Tehnologii. 2007. №4. S. 6–10.
13. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
14. Kablov E.N. Aviatsionnoe materialovedenie v XXI veke. Perspektivy i zadachi [Aviation materials science in the XXI century. Perspectives and tasks] // Aviatsionnye materialy. Izbrannye trudy «VIAM» 1932–2002. M.: VIAM, 2002. S. 23–47.
15. Grashhenkov D.V., Chursova L.V. Strategiya razvitiya kompozicionnyh i funkcionalnyh materialov [Strategy of development of composite and functional materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 231–242.
2. Petrova A.P. Povyshenie termostojkosti poliuretanovyh klejashhih sistem pri modifikacii karboranami [Increase of thermal stability of polyurethane gluing systems when updating by carboranes] // Novosti materialovedenija. Nauka i tehnika: jelektron. nauch.-tehnich. zhurn. 2017. №1. St. 04. Available at: http://www.materialsnews.ru (accessed: June 27, 2017).
3. Petrova A.P., Laptev A.B. Termicheskaja ustojchivost karboransoderzhashhih poliuretanovyh klejashhih sistem [Thermal stability carborane of containing polyurethane gluing systems] // Klei. Germetiki. Tehnologii. 2017. №8. S. 2–5.
4. Lipatova T.Je., Bakalo L.A. Kinetika i mehanizm reakcij obrazovanija poliuretanov [Kinetics and mechanism of reactions of education poliuretanov] // Uspehi himii poliuretanov. Kiev: Naukova Dumka, 1972. S. 195–213.
5. Valeckij P.M., Petrova A.P. Polimernye klei na osnove karboransoderzhashhih soedinenij [Polymeric glues on basis carborane of containing connections] // Klei. Germetiki. Tehnologii. 2005. №3. S. 2–5.
6. Lukina N.F., Dementeva L.A., Petrova A.P., Serezhenkov A.A. Konstrukcionnye i termostojkie klei [Constructional and heat-resistant glues] // Aviacionnye materialy i tehnologii. 2012. №S. S. 328–335.
7. Sharova I.A., Petrova A.P. Obzor po materialam mezhdunarodnoj konferencii po kleyam i germetikam (WAC-2012, Franciya) [Review of world adhesive and sealant conference (WAC-2012, France] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №8. St. 06. Available at: http://www.viam-works.ru (accessed: June 19, 2017).
8. Petrova A.P. Magnitoprovodjashhie kleevye kompozicii na osnove karboransoderzhashhih soedinenij [Magneto carrying-out glue compositions on basis carborane of containing connections] // Klei. Germetiki. Tehnologii. 2006. №11. S. 3–4.
9. Petrova A.P. Povyshenie termostojkosti klejashhih sistem na osnove fenolformaldegidnyh oligomerov pri modifikacii karboranami [Increasing thermal resistance of the adhesive systems based on phenol-formaldehyde oligomers with modification of the carborane] // Novosti materialovedenija. Nauka i tehnika: jelektron. nauch.-tehnich. zhurn. 2017. №1. St. 03. Available at: http://www.materialsnews.ru (accessed: June 27, 2017).
10. Petrova A.P. Laptev A.B. Termicheskaja ustojchivost karboransoderzhashhih klejashhih sistem na osnove fenolformaldegidnyh oligomerov [Thermal stability of karboransoderzhashchy gluing systems on the basis of fenolformaldegidny oligomers] // Klei. Germetiki. Tehnologii. 2017. №7. S. 2–6.
11. Petrova A.P., Laptev A.B. Fenolno-kauchukovye klei, modificirovannye karboranami [The phenolic and rubber glues modified by carboranes] // Klei. Germetiki. Tehnologii. 2017. №6. S. 2–6.
12. Petrova A.P., Valeckij P.M. Fenolno-kauchukovye karboransoderzhashhie klei s sobstvennym fer-romagnetizmom [Phenolic and rubber carborane containing glues with own ferromagnetizm] // Klei. Germetiki. Tehnologii. 2007. №4. S. 6–10.
13. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
14. Kablov E.N. Aviatsionnoe materialovedenie v XXI veke. Perspektivy i zadachi [Aviation materials science in the XXI century. Perspectives and tasks] // Aviatsionnye materialy. Izbrannye trudy «VIAM» 1932–2002. M.: VIAM, 2002. S. 23–47.
15. Grashhenkov D.V., Chursova L.V. Strategiya razvitiya kompozicionnyh i funkcionalnyh materialov [Strategy of development of composite and functional materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 231–242.
8.
category: Testing of materials and structures
УДК 678.06:629.7
Naumov I.S.1, Petrova A.P.1, Barinov D.Ya.1
THERMOGRAVIMETRIC ANALYSIS OF SEALING RUBBERS WITH THE LOWERED COMBUSTIBILITY IN THE ENVIRONMENT OF INERT GAS(ARGON)
Thermogravimetric analysis in argon environment of rubbers of sealing assignment, including the rubbers possessing lowered combustibility both in the initial condition, and with addition of finely dispersed flame retardants is carried out. Influence of used flame retardants on thermogravimetric characteristics of the received rubbers with the lowered combustibility is investigated.
Keywords: organic silicon and ethylenepropylene-diene rubbers, flame retardant, combustibility, aluminum hydroxide, magnesium hydroxide, decabromdiphenyl oxide, TGM-analysis.
Reference List
1. Kablov E.N. Materialy novogo pokolenija – osnova innovacij, tehnologicheskogo liderstva i nacionalnoj bezopasnosti Rossii [Materials of new generation – basis of innovations, technological leadership and national security of Russia] // Intellekt i tehnologii. 2016. №2 (14). S. 16–21.
2. Kablov E.N. Khimiya v aviatsionnom materialovedenii [Chemistry in aviation materials science] // Rossiyskiy khimicheskiy zhurnal. 2010. T. LIV. №1. S. 3–4.
3. Kablov E.N. Shestoy tekhnologicheskiy uklad [Sixth technological way] // Nauka i zhizn. 2010. №4. S. 2–7.
4. Istorija aviacionnogo materialovedenija. VIAM – 80 let: gody i ljudi [History of aviation materials science. VIAM – 80 years: years and people] / pod obshh. red. E.N. Kablova. M.: VIAM, 2012. S. 346–348.
5. Kablov E.N. Aviatsionnoe materialovedenie v XXI veke. Perspektivy i zadachi [Aviation materials science in the XXI century. Perspectives and tasks] // Aviatsionnye materialy. Izbrannye trudy «VIAM» 1932–2002. M.: VIAM, 2002. S. 23–47.
6. Naumov I.S., Petrova A.P., Chajkun A.M. Reziny uplotnitel'nogo naznachenija i snizhenie ih gorjuchesti [Rubbers of sealing assignment and decrease in their combustibility] // Vse materialy. Jenciklopedicheskij spravochnik. 2013. №5. S. 28–35.
7. Chaikun A.M., Eliseev O.A., Naumov I.S., Venediktova M.A. Osobennosti morozostojkih rezin na osnove razlichnyh kauchukov [Features of old-resistant rubbers on the basis on different unvulcanized rubbers] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №12. St. 04. Available at: http://www.viam-works.ru (accessed: December 05, 2017).
8. Naumov I.S., Petrova A.P., Eliseev O.A., Barbotko S.L. Eksperimentalnye issledovaniya v oblasti sozdaniya kremnijorganicheskih rezin s ponizhennoj goryuchestyu [Experimental research in the field of development of organic silicon rubbers with low flammability] //Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №10. St. 09 Available at: http://www.viam-works.ru (accessed: December 05, 2017). DOI: 10.18577/2307-6046-2015-0-10-9-9.
9. Alifanov E.V., Chaykun A.М., Venediktova M.A., Naumov I.S. Osobennosti receptur rezin na osnove etilenpropilenovyh kauchukov i ih primenenie v izdeliyah specialnogo naznacheniya (obzor) [Specialties of rubber compounds recipes based on ethylene-propylene rubbers and their application in the articles for special purpose (review)] //Aviacionnye materialy i tehnologii. 2015. №2 (35). S. 51–55. DOI: 10.18577/2071-9140-2015-0-2-51-55.
10. Naumov I.S., Petrova A.P., Barbot'ko S.L., Chajkun A.M. i dr. Cvetnye i chernye uplotnitel'nye reziny ponizhennoj gorjuchesti na osnove siloksanovyh kauchukov [Color and black sealing rubbers of the lowered combustibility on the basis of siloxane rubbers ] // Vse materialy. Jenciklopedicheskij spravochnik. 2017. №5. S. 24–31.
11. Naumov I.S., Petrova A.P., Barbotko S.L., Guliaev A.I. Reziny s ponizhennoi goriuchestiu na osnove etilenpropilen-dienovogo kauchuka [Rubbers with the lowered combustibility on basis of ethylenepropylene-diene rubber] // Trudy VIAM: elektron. nauch.-tekhnich. zhurn. 2016. №2. St. 09. Available at: http://www.viam-works.ru (accessed: December 05, 2017). DOI: 10.18577/2307-6046-2016-0-2-9-9.
12. Naumov I.S., Marahovskij P.S., Petrova A.P., Barinov D.Ja. Termogravimetricheskij analiz uplotnitel'nyh rezin ponizhennoj gorjuchesti v srede vozduha [Thermogravimetric analysis of sealing rubbers with the lowered combustibility in the environment of air] // Novosti materi-alovedenija. Nauka i tehnika: jelektron. nauch.-tehnich. zhurn. 2017. №1 (25). St. 07. URL: http://www.materialsnews.ru (accessed: December 05, 2017).
13. Bolshoy spravochnik rezinshchika v 2 ch [The big reference book for specialist in rubbers in 2 p.]. M.: Tekhinform, 2012. 1385 s.
14. Tehnologija reziny: recepturostroenie i ispytanija. Per. s angl. [Technology of rubber: retsepturostroyeniye and tests. Trans. from Engl.] / pod red. Dzh.S. Dika. SPb.: Nauchnye osnovy i tehnologii, 2010. 620 s.
15. Gorenie, destrukcija i stabilizacija polimerov [Burning, destruktsiya and stabilization of polymers] / pod red. G.E. Zaikova. SPb.: Nauchnye osnovy i tehnologii, 2008. 422 s.
16. Normy letnoj godnosti samoletov transportnoj kategorii [Standards of the flight validity of airplanes of transport category]: AP-25: utv. Postanovleniem 28-j Sessii po aviacii i ispolzovaniju vozdushnogo prostranstva 11.12.2008. 3-e izd. s popravkami 1–6. M.: Aviaizdat, 2009. 274 s.
2. Kablov E.N. Khimiya v aviatsionnom materialovedenii [Chemistry in aviation materials science] // Rossiyskiy khimicheskiy zhurnal. 2010. T. LIV. №1. S. 3–4.
3. Kablov E.N. Shestoy tekhnologicheskiy uklad [Sixth technological way] // Nauka i zhizn. 2010. №4. S. 2–7.
4. Istorija aviacionnogo materialovedenija. VIAM – 80 let: gody i ljudi [History of aviation materials science. VIAM – 80 years: years and people] / pod obshh. red. E.N. Kablova. M.: VIAM, 2012. S. 346–348.
5. Kablov E.N. Aviatsionnoe materialovedenie v XXI veke. Perspektivy i zadachi [Aviation materials science in the XXI century. Perspectives and tasks] // Aviatsionnye materialy. Izbrannye trudy «VIAM» 1932–2002. M.: VIAM, 2002. S. 23–47.
6. Naumov I.S., Petrova A.P., Chajkun A.M. Reziny uplotnitel'nogo naznachenija i snizhenie ih gorjuchesti [Rubbers of sealing assignment and decrease in their combustibility] // Vse materialy. Jenciklopedicheskij spravochnik. 2013. №5. S. 28–35.
7. Chaikun A.M., Eliseev O.A., Naumov I.S., Venediktova M.A. Osobennosti morozostojkih rezin na osnove razlichnyh kauchukov [Features of old-resistant rubbers on the basis on different unvulcanized rubbers] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №12. St. 04. Available at: http://www.viam-works.ru (accessed: December 05, 2017).
8. Naumov I.S., Petrova A.P., Eliseev O.A., Barbotko S.L. Eksperimentalnye issledovaniya v oblasti sozdaniya kremnijorganicheskih rezin s ponizhennoj goryuchestyu [Experimental research in the field of development of organic silicon rubbers with low flammability] //Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №10. St. 09 Available at: http://www.viam-works.ru (accessed: December 05, 2017). DOI: 10.18577/2307-6046-2015-0-10-9-9.
9. Alifanov E.V., Chaykun A.М., Venediktova M.A., Naumov I.S. Osobennosti receptur rezin na osnove etilenpropilenovyh kauchukov i ih primenenie v izdeliyah specialnogo naznacheniya (obzor) [Specialties of rubber compounds recipes based on ethylene-propylene rubbers and their application in the articles for special purpose (review)] //Aviacionnye materialy i tehnologii. 2015. №2 (35). S. 51–55. DOI: 10.18577/2071-9140-2015-0-2-51-55.
10. Naumov I.S., Petrova A.P., Barbot'ko S.L., Chajkun A.M. i dr. Cvetnye i chernye uplotnitel'nye reziny ponizhennoj gorjuchesti na osnove siloksanovyh kauchukov [Color and black sealing rubbers of the lowered combustibility on the basis of siloxane rubbers ] // Vse materialy. Jenciklopedicheskij spravochnik. 2017. №5. S. 24–31.
11. Naumov I.S., Petrova A.P., Barbotko S.L., Guliaev A.I. Reziny s ponizhennoi goriuchestiu na osnove etilenpropilen-dienovogo kauchuka [Rubbers with the lowered combustibility on basis of ethylenepropylene-diene rubber] // Trudy VIAM: elektron. nauch.-tekhnich. zhurn. 2016. №2. St. 09. Available at: http://www.viam-works.ru (accessed: December 05, 2017). DOI: 10.18577/2307-6046-2016-0-2-9-9.
12. Naumov I.S., Marahovskij P.S., Petrova A.P., Barinov D.Ja. Termogravimetricheskij analiz uplotnitel'nyh rezin ponizhennoj gorjuchesti v srede vozduha [Thermogravimetric analysis of sealing rubbers with the lowered combustibility in the environment of air] // Novosti materi-alovedenija. Nauka i tehnika: jelektron. nauch.-tehnich. zhurn. 2017. №1 (25). St. 07. URL: http://www.materialsnews.ru (accessed: December 05, 2017).
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9.
category: Testing of materials and structures
УДК 669.018.44:620.178.322.2
Belyaev M.S.1, Gorbovets M.A.1, Shvedov V.A.1
THE INFLUENCE OF TEST CONDITIONS ON THE LOW CYCLE FATIGUE AND PARAMETERS OF CYCLIC DEFORMATION OF SUPERALLOY VZH175
Investigation of low-cycle fatigue of superalloy VZh175 held at a given total strain Δεt and temperatures 20, 650, 750°С. Smooth samples with a diameter of 5,0 mm has been tested at a loading frequency of 1 Hz on the basis of 104 cycles.
Analyzed the change of the loops of the elastic-plastic hysteresis depending on the number of cycles and test temperature. Width of the hysteresis loop εin ambiguous varies with temperature.
The middle line of low cycle fatigue is built and the values of the endurance limits determined. Most high limit of LCF superalloy VZh175 has at room temperature. Also characteristics of LCF determined by the accumulated strain εn.
Keywords: low сycle fatigue (LCF), elastic-plastic hysteresis, inelastic deformation, characteristics of LCF, superalloy VZh175.
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